- Experience in organic synthesis: routine synthesis, identification and purification of compounds using various spectroscopic and purification techniques.
- Experience working on small molecule activation, utilising classical organic and electro synthetic techniques.
- 8 Years’ experience demonstrating chemistry for undergraduate students in the university.
- Use of a wide variety of synthetic organic chemistry techniques along with the associated spectroscopic analysis.
Apr, 2021 - Sekarang
•
3 tahun, 5 bulan
Pendidikan
Damietta University
2011 - 2015
•
4 tahun
Master of Chemistry
Egypt
2011 - 2015
•
4 tahun
Damietta University
2006 - 2010
•
4 tahun
Bachelor of Chemistry
Egypt
2006 - 2010
•
4 tahun
Penerbitan
Selective Electrosynthetic Hydrocarboxylation of α,β-Unsaturated Esters with Carbon Dioxide
Electrosynthetic hydrocarboxylation of α,β-unsaturated olefins with excellent regioselectivity is reported. The method requires no sacrificial electrode and is thus amenable to a flow configuration. The products are purified by simple crystallization. The synthesis of a precursor to ethosuximide, which contains an all-carbon quaternary centre, illustrates the potential of the process. Finally, a robustness study has benchmarked the process for future users.
Selective α,δhydrocarboxylation of conjugated dienes utilizing CO2 and electrosynthesis
We report a new electrosynthetic approach, that does not rely on a sacrificial electrode, the reported method allows unprecedented direct access to carboxylic acids derived from dienes at the δ-position. In addition, the α,δ-dicarboxylic acid or the α,δ-reduced alkene can be easily accessed by simple modification of the reaction conditions.
preparation of 2-amino-6-chloropyridine-3,5-dicarbonitrile
A green one-pot method for efficient synthesis of 2-amino-6-chloropyridine-3,5-dicarbonitrile derivatives was developed, based on stirring of various aldehydes and malononitrile with tetrachlorosilane and zinc chloride under solvent-free conditions at room temperature for 3–10 h. The effects of zinc chloride and the reaction conditions were studied. Compounds were characterized by X-ray analysis and NMR spectroscopy.
Pengesahan
Tepat pada masa
100%
Mengikut bajet
100%
Kadar terima
100%
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